Total synthesis of TMG-chitotriomycin based on an automated electrochemical assembly of a disaccharide building block
In: Beilstein Journal of Organic Chemistry, Jg. 13 (2017), Heft 1, S. 919-924
Online
academicJournal
Zugriff:
The total synthesis of TMG-chitotriomycin using an automated electrochemical synthesizer for the assembly of carbohydrate building blocks is demonstrated. We have successfully prepared a precursor of TMG-chitotriomycin, which is a structurally-pure tetrasaccharide with typical protecting groups, through the methodology of automated electrochemical solution-phase synthesis developed by us. The synthesis of structurally well-defined TMG-chitotriomycin has been accomplished in 10-steps from a disaccharide building block.
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Total synthesis of TMG-chitotriomycin based on an automated electrochemical assembly of a disaccharide building block
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Autor/in / Beteiligte Person: | Isoda, Yuta ; Sasaki, Norihiko ; Kitamura, Kei ; Takahashi, Shuji ; Manmode, Sujit ; Takeda-Okuda, Naoko ; Tamura, Jun-ichi ; Nokami, Toshiki ; Itoh, Toshiyuki |
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Zeitschrift: | Beilstein Journal of Organic Chemistry, Jg. 13 (2017), Heft 1, S. 919-924 |
Veröffentlichung: | Beilstein-Institut, 2017 |
Medientyp: | academicJournal |
ISSN: | 1860-5397 (print) |
DOI: | 10.3762/bjoc.13.93 |
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