Short-RInChIKey=SA-FUHFF-UHFFFADPSC-XDOHQPHWJL-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ ... : Short-RInChIKey=SA-FUHFF-UAOMNDAJRK-XDOHQPHWJL-HMWSWNZYAQ-NUHFF-NUHFF-NUHFF-ZZZ ...
chemotion-repository, 2024
academicJournal
Zugriff:
4-Bromo-1-(4-bromo-2-hydroxynaphthalen-1-yl)naphthalen-2-ol (238 mg, 536 μmol, 1.00 equiv) and copper(I) cyanide (192 mg, 2.14 mmol, 4.00 equiv) were dissolved N,N-dimethylformamide (3.8 mL), and the mixture was degassed by bubbling with N2 for 15 minutes. The mixture was heated with stirring to reflux for 17 hours. The residue was extracted with ethyl acetate (3 x 20 mL). The pH was checked to see if it was in the 5-6 range. As it was 6, no further reagents were added.. The combined organic layers were washed with water (50 mL) and brine (50 mL), dried over Na2SO4, filtered, and the solvent was evaporated under reduced pressure. ...
Titel: |
Short-RInChIKey=SA-FUHFF-UHFFFADPSC-XDOHQPHWJL-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ ... : Short-RInChIKey=SA-FUHFF-UAOMNDAJRK-XDOHQPHWJL-HMWSWNZYAQ-NUHFF-NUHFF-NUHFF-ZZZ ...
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Autor/in / Beteiligte Person: | Sengpiel, Tobias |
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Veröffentlichung: | chemotion-repository, 2024 |
Medientyp: | academicJournal |
DOI: | 10.14272/reaction/sa-fuhff-uhfffadpsc-xdohqphwjl-uhfffadpsc-nuhff-nuhff-nuhff-zzz.1 |
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