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During last few decades, oligochitosan (OCS)-coated nanoparticles have received great interest for nanomedicine, food and environment applications. However, their current formulation techniques are time-consuming with multi-synthesis/purification steps and sometimes require the use of organic solvents, crosslinkers and surfactants. Herein, we report a facile and rapid one-pot synthesis of OCS-based nanoparticles using photo-initiated reversible addition fragmentation chain transfer polymerization-induced self-assembly (Photo-RAFT PISA) under UV-irradiation at room temperature. To achieve this, OCS was first functionalized by a chain transfer agent (CTA) resulting in a macromolecular chain transfer agent (OCS-CTA), which will act as a reactive electrostatic/steric stabilizer. Owing to its UV-sensitivity, OCS-CTA was then used as photo-iniferter to initiate the polymerization of 2-hydroxypropyl methacrylate (HPMA) in aqueous acidic buffer, resulting in OCS-g-PHPMA amphiphilic grafted copolymers which self-assemble into nano-objects. Transmission electron microscopy and light scattering analysis reveal formation of spherical nanostructures.

Titel:	One-pot Formulation of Cationic Oligochitosan Coated Nanoparticles via Photo- Polymerization Induced Self-Assembly.
Autor/in / Beteiligte Person:	Oumerri, J ; Qayouh, H ; Arteni, AA ; Six, JL ; Lahcini, M ; Ferji, K
Link:	Zum Volltext
Zeitschrift:	Chemphyschem : a European journal of chemical physics and physical chemistry, 2024-04-22, S. e202400291
Veröffentlichung:	Ahead of Print, 2024
Medientyp:	academicJournal
ISSN:	1439-7641 (electronic)
DOI:	10.1002/cphc.202400291
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Grant Information: Campus France Contributed Indexing: Keywords: Nano-objects; cationic nanoparticles; polymerization; polysaccharide; self-assembly Entry Date(s): Date Created: 20240422 Latest Revision: 20240518 Update Code: 20240518

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One-pot Formulation of Cationic Oligochitosan Coated Nanoparticles via Photo- Polymerization Induced Self-Assembly.